**** SECTION 1 - CHEMICAL PRODUCT AND COMPANY IDENTIFICATION ****

MSDS Name: Ammonium Sulfide Solution
Catalog Numbers:
    S70789, A705 250, A705 500, A705225, A705250, A705500
Synonyms:
    Diammonium sulfide; Ammonium monosulfide; Ammonium sulfide ((NH4)2S).
Company Identification:  Fisher Scientific
                        1 Reagent Lane
                        Fairlawn, NJ  07410
For information, call:  201-796-7100
Emergency Number:       201-796-7100
For CHEMTREC assistance, call: 800-424-9300
For International CHEMTREC assistance, call: 703-527-3887

         **** SECTION 2 - COMPOSITION, INFORMATION ON INGREDIENTS ****

+----------------+--------------------------------------+----------+-----------+
|      CAS#      |              Chemical Name           |    %     |  EINECS#  |
|----------------|--------------------------------------|----------|-----------|
|     7732-18-5  |Water                                 |  76-80   | 231-791-2 |
|----------------|--------------------------------------|----------|-----------|
|    12135-76-1  |Ammonium sulfide                      |  20-24   | 235-223-4 |
+----------------+--------------------------------------+----------+-----------+
         Hazard Symbols: T C
         Risk Phrases: 10 21 23/25 34

                 **** SECTION 3 - HAZARDS IDENTIFICATION ****

                              EMERGENCY OVERVIEW
Appearance:  yellow. Flash Point: 140 deg F.
Danger! Flammable liquid and vapor. Harmful if inhaled. May be
harmful if absorbed through the skin. Corrosive. Harmful if
swallowed. Causes eye and skin burns. Causes digestive and
respiratory tract burns.
Target Organs: Lungs, eyes, nervous system, skin, mucous membranes.

Potential Health Effects
    Eye:
         Causes eye burns.
    Skin:
         Causes skin burns. May be absorbed through the skin in harmful
         amounts. Chronic exposure may cause low blood pressure, persistent
         cough, and weight loss.
    Ingestion:
         Causes gastrointestinal tract burns.
    Inhalation:
         May cause severe irritation of the respiratory tract with sore
         throat, coughing, shortness of breath and delayed lung edema.
    Chronic:
         Chronic exposure may cause low blood pressure, persistent cough, and
         weight loss.

                   **** SECTION 4 - FIRST AID MEASURES ****

    Eyes:
         Immediately flush eyes with plenty of water for at least 15 minutes,
         occasionally lifting the upper and lower eyelids. Get medical aid
         immediately.
    Skin:
         Get medical aid immediately. Immediately flush skin with plenty of
         soap and water for at least 15 minutes while removing contaminated
         clothing and shoes.
    Ingestion:
         Do NOT induce vomiting. If victim is conscious and alert, give 2-4
         cupfuls of milk or water. Never give anything by mouth to an
         unconscious person. Get medical aid immediately.
    Inhalation:
         Remove from exposure to fresh air immediately. If not breathing,
         give artificial respiration. If breathing is difficult, give oxygen.
         Get medical aid.
    Notes to Physician:
         Treat symptomatically and

                 **** SECTION 5 - FIRE FIGHTING MEASURES ****

    General Information:
         Vapors may form an explosive mixture with air. Use water spray to
         keep fire-exposed containers cool. Wear appropriate protective
         clothing to prevent contact with skin and eyes. Wear a self-contained
         breathing apparatus (SCBA) to prevent contact with thermal
         decomposition products. Containers may explode in the heat of a
         fire. Flammable liquid and vapor.
    Extinguishing Media:
         For small fires, use dry chemical, carbon dioxide, water spray or
         alcohol-resistant foam.
    Autoignition Temperature:Not available.
    Flash Point:           Not available.
    Explosion Limits, lower:Not available.
    Explosion Limits, upper:Not available.
    NFPA Rating: (estimated) Health: 3; Flammability: 2; Reactivity: 0

               **** SECTION 6 - ACCIDENTAL RELEASE MEASURES ****

    General Information: Use proper personal protective equipment as indicated
                         in Section 8.
    Spills/Leaks:
         Absorb spill with inert material (e.g. vermiculite, sand or earth),
         then place in suitable container. Remove all sources of ignition.
         Provide ventilation. Approach spill from upwind.

                  **** SECTION 7 - HANDLING and STORAGE ****

    Handling:
         Wash thoroughly after handling. Use with adequate ventilation.
         Loosen closure cautiously before opening. Do not get in eyes, on
         skin, or on clothing. Empty containers retain product residue,
         (liquid and/or vapor), and can be dangerous. Keep container tightly
         closed. Do not ingest or inhale. Do not pressurize, cut, weld, braze,
         solder, drill, grind, or expose empty containers to heat, sparks or
         open flames.
    Storage:
         Keep away from heat, sparks, and flame. Store in a tightly closed
         container. Store in a cool, dry, well-ventilated area away from
         incompatible substances. Flammables-area.

         **** SECTION 8 - EXPOSURE CONTROLS, PERSONAL PROTECTION ****

    Engineering Controls:
         Facilities storing or utilizing this material should be equipped
         with an eyewash facility and a safety shower. Use adequate general or
         local exhaust ventilation to keep airborne concentrations below the
         permissible exposure limits.

                                Exposure Limits
+--------------------+-------------------+-------------------+-----------------+
|   Chemical Name    |        ACGIH      |       NIOSH       |OSHA - Final PELs|
|--------------------|-------------------|-------------------|-----------------|
| Water              |none listed        |none listed        |none listed      |
|--------------------|-------------------|-------------------|-----------------|
| Ammonium sulfide   |none listed        |none listed        |none listed      |
+--------------------+-------------------+-------------------+-----------------+

    OSHA Vacated PELs:
         Water:
            No OSHA Vacated PELs are listed for this chemical.
         Ammonium sulfide:
            No OSHA Vacated PELs are listed for this chemical.

    Personal Protective Equipment

                Eyes:
                      Wear chemical goggles.
                Skin:
                      Wear appropriate gloves to prevent skin exposure.
            Clothing:
                      Wear appropriate protective clothing to prevent skin
                      exposure.
         Respirators:
                      Follow the OSHA respirator regulations found in 29CFR
                      1910.134 or European Standard EN 149. Always use a
                      NIOSH or European Standard EN 149 approved respirator
                      when necessary.

            **** SECTION 9 - PHYSICAL AND CHEMICAL PROPERTIES ****

Physical State:             Liquid
Appearance:                 yellow
Odor:                       sulfurous odor
pH:                         Not available.
Vapor Pressure:             Not available.
Vapor Density:              >1
Evaporation Rate:           Not available.
Viscosity:                  Not available.
Boiling Point:              Not available.
Freezing/Melting Point:     Not available.
Decomposition Temperature:  Not available.
Solubility in water:        Soluble in water.
Specific Gravity/Density:   Not available.
Molecular Formula:          (NH4)2S
Molecular Weight:           68.15

                **** SECTION 10 - STABILITY AND REACTIVITY ****

    Chemical Stability:
         Stable under normal temperatures and pressures.
    Conditions to Avoid:
         Incompatible materials, ignition sources, excess heat.
    Incompatibilities with Other Materials:
         Contact with strong oxidizers may cause fire. Incompatible with
         alkalies, strong acids, copper, brass, bronze, strong bases, zinc,
         and aluminum. Contact with incompatible materials may release
         poisonous and flammable hydrogen sulfide gas.
    Hazardous Decomposition Products:
         Nitrogen oxides, oxides of sulfur, ammonia and/or derivatives,
         hydrogen sulfide.
    Hazardous Polymerization: Has not been reported.

               **** SECTION 11 - TOXICOLOGICAL INFORMATION ****

    RTECS#:
         CAS# 7732-18-5: ZC0110000
         CAS# 12135-76-1 unlisted.
    LD50/LC50:
         CAS# 7732-18-5: Oral, rat: LD50 = >90 mL/kg.
         CAS# 12135-76-1.
    Carcinogenicity:
      Water -
         Not listed by ACGIH, IARC, NIOSH, NTP, or OSHA.
      Ammonium sulfide -
         Not listed by ACGIH, IARC, NIOSH, NTP, or OSHA.
    Epidemiology:
         No data available.
    Teratogenicity:
         No data available.
    Reproductive Effects:
         No data available.
    Neurotoxicity:
         No data available.
    Mutagenicity:
         No data available.
    Other Studies:
         No data available.

                 **** SECTION 12 - ECOLOGICAL INFORMATION ****
 
 

                **** SECTION 13 - DISPOSAL CONSIDERATIONS ****

Chemical waste generators must determine whether a discarded chemical
is classified as a hazardous waste.
US EPA guidelines for the classification determination are listed in
40 CFR Parts 261.3. Additionally, waste generators must consult state
and local hazardous waste regulations to ensure complete and accurate
classification.
RCRA P-Series: None listed.
RCRA U-Series: None listed.

                 **** SECTION 14 - TRANSPORT INFORMATION ****

    US DOT
         Shipping Name: (TOXIC), AMMONIUM SULFIDE SOLUTION
          Hazard Class: 8
             UN Number: UN2683
         Packing Group: II
    Canadian TDG
         Shipping Name: AMMONIUM SULFIDE
          Hazard Class: 8(3.6)(19.2)
             UN Number: UN2683

                 **** SECTION 15 - REGULATORY INFORMATION ****

US FEDERAL
    TSCA
         CAS# 7732-18-5 is listed on the TSCA inventory.
         CAS# 12135-76-1 is listed on the TSCA inventory.
       Health & Safety Reporting List
         None of the chemicals are on the Health & Safety Reporting List.
       Chemical Test Rules
         None of the chemicals in this product are under a Chemical Test Rule.
       Section 12b
         None of the chemicals are listed under TSCA Section 12b.
       TSCA Significant New Use Rule
         None of the chemicals in this material have a SNUR under TSCA.
    SARA
       Section 302 (RQ)
         CAS# 12135-76-1: final RQ = 100 pounds (45.4 kg)
       Section 302 (TPQ)
         None of the chemicals in this product have a TPQ.
       SARA Codes
         CAS # 12135-76-1: acute, flammable, reactive.
       Section 313
         No chemicals are reportable under Section 313.
    Clean Air Act:
         This material does not contain any hazardous air pollutants.
         This material does not contain any Class 1 Ozone depletors.
         This material does not contain any Class 2 Ozone depletors.
    Clean Water Act:
         CAS# 12135-76-1 is listed as a Hazardous Substance under the CWA.
         None of the chemicals in this product are listed as Priority
         Pollutants under the CWA.
         None of the chemicals in this product are listed as Toxic Pollutants
         under the CWA.
    OSHA:
         None of the chemicals in this product are considered highly hazardous
         by OSHA.
STATE
    Water is not present on state lists from CA, PA, MN, MA, FL, or NJ.
    Ammonium sulfide can be found on the following state right to know
    lists: California, New Jersey, Pennsylvania, Massachusetts.
    California No Significant Risk Level:
    None of the chemicals in this product are listed.
European/International Regulations
    European Labeling in Accordance with EC Directives
         Hazard Symbols: T C
         Risk Phrases:
                      R 10  Flammable.
                      R 21  Harmful in contact with skin.
                      R 23/25  Toxic by inhalation and if swallowed.
                      R 34  Causes burns.
         Safety Phrases:
  WGK (Water Danger/Protection)
         CAS# 7732-18-5: No information available.
         CAS# 12135-76-1: 2
  United Kingdom Occupational Exposure Limits

  Canada
         CAS# 7732-18-5 is listed on Canada's DSL List.
         CAS# 12135-76-1 is listed on Canada's DSL List.
         This product has a WHMIS classification of B3, D1B, E.
         CAS# 7732-18-5 is not listed on Canada's Ingredient Disclosure List.
         CAS# 12135-76-1 is not listed on Canada's Ingredient Disclosure List.
  Exposure Limits

                 **** SECTION 16 - ADDITIONAL INFORMATION ****

    MSDS Creation Date:  9/02/1997  Revision #3 Date:  3/15/2001

    The information above is believed to be accurate and represents the best
    information currently available to us. However, we make no warranty of
    merchantability or any other warranty, express or implied, with respect to
    such information, and we assume no liability resulting from its use. Users
    should make their own investigations to determine the suitability of the
    information for their particular purposes. In no way shall the company be
    liable for any claims, losses, or damages of any third party or for lost
    profits or any special, indirect, incidental, consequential or exemplary
    damages, howsoever arising, even if the company has been advised of
    the possibility of such damages.